Showing 50 of 25357 papers

Quality Control of High-Speed Steel Drills Tempered under Various Conditions

A. E. Kameristov, N. S. Kilkov, E. S. Sergeeva, N. P. Sidorova
1975 SovietRxiv: ru-197501.13037

This study evaluates the quality of high-speed steel drills subjected to several industrial tempering schedules, comparing standard triple tempering with shorter double-tempering treatments used on plant equipment. Drills made from R18, R6M3, and R6M5 steels were tested for hardness, microstructure,…

On Methods for Determining the Dependence of Changes in the Properties of Hardened Steels on Temperature-Time Exposure During Tempering

Yu. M. Lozinskii, I. T. Tikhonov
1975 SovietRxiv: ru-197501.13036

This paper critiques the Hollomon and Jaffe time temperature parameter for describing changes in hardened steel properties during tempering, arguing that its assumptions about activation energy and process constants are theoretically and practically problematic. The authors propose using the classic…

Hardening of iron-cobalt-tungsten alloys during two-stage tempering

A. D. Klement’ev
1975 SovietRxiv: ru-197501.13034

This paper examines hardening behavior in a precipitation-hardening iron-cobalt-tungsten alloy during two-stage tempering, using hardness measurements on an alloy containing 25 percent cobalt and 25 percent tungsten. By comparing single-stage tempering with preliminary low-temperature tempering foll…

On the Issue of Students’ Independent Work in Descriptive Geometry

B. L. Stepanov, V. A. Voskresenskii
1975 SovietRxiv: ru-197501.12969

This article examines the organization and workload of students’ independent homework in a descriptive geometry course at a technical institute. Using time studies conducted in selected student groups in the 1966/67 and 1969/70 academic years, the authors compare the time required for weekly and maj…

From the Experience of Compiling Methodological Guides on Descriptive Geometry

L. S. Skriptsov, V. A. Voskresensky
1975 SovietRxiv: ru-197501.12968

The article addresses the need for methodological guides to support full-time students’ independent completion of large homework assignments in descriptive geometry, given limited classroom time for detailed explanation. Drawing on the experience of the Department of Descriptive Geometry at Tomsk Po…

Issues in the History of Axonometry

V. A. Voskresenskii
1975 SovietRxiv: ru-197501.12967

This article argues for the historical study of axonometry as a major branch of descriptive geometry, understood in connection with both mathematics and technology. Reviewing Soviet discussions on the history of science and surveying textbooks, monographs, dissertations, and historical works on engi…

On the Development of Axonometry in the USSR

V. A. Voskresenskii
1975 SovietRxiv: ru-197501.12964

This article surveys Soviet research on axonometry from the mid 1950s through the 1960s, emphasizing developments that followed earlier accounts of parallel and central axonometric projection. It reviews theoretical work on Pohlke’s theorem, distortion coefficients, curvilinear and panoramic axonome…

On Some Works in the Field of Axonometry

V. A. Voskresenskii
1975 SovietRxiv: ru-197501.12962

This article surveys selected Soviet work on axonometry, with particular attention to the Kruppa problem and the fundamental theorem of central axonometry. It compares synthetic, metric, coordinate, and multidimensional approaches by authors including Kotov, Ryunk, Pervikova, Manevich, Beskin, Borod…

Categories of Research in the Field of Russian Axonometry

V. A. VOSKRESENSKII
1975 SovietRxiv: ru-197501.12960

This paper surveys research on axonometry in Russia and the Soviet Union, arguing that the field should not be defined primarily by visual clarity but by coordinate-based parallel or central representation constructed at a specified axonometric scale. It reviews the emergence of axonometric projecti…

Effect of Alkali Metal Hydroxides on the Granulation of Active Magnesium Oxide

I. N. Lantsman, P. D. Khalfina, V. M. Vityugin, N. F. Stas
1975 SovietRxiv: ru-197501.12938

This study examines how alkali metal hydroxide additives affect the granulation, mechanical strength, and carbon dioxide adsorption properties of active magnesium oxide prepared from basic magnesium carbonate. Magnesium carbonate mixtures containing sodium, potassium, lithium, rubidium, or cesium hy…

Studies on the Granulation of Adsorbents Based on Magnesium Oxide with Clay Binders

I. N. Lantsman, P. D. Khalfina, V. M. Vityugin, N. F. Stas
1975 SovietRxiv: ru-197501.12937

This study examines the use of clay binders to granulate magnesium oxide based adsorbents, addressing problems associated with powdered sorbents such as low bed permeability, entrainment, and caking. Granules prepared from magnesium carbonate containing potassium hydroxide were formed on a laborator…

Some Acyl Derivatives of 1-Benzylsemicarbazide

A. G. Pechenkin, I. G. Fedkova, Z. M. Murav’eva
1975 SovietRxiv: ru-197501.12936

This paper reports the synthesis of previously undescribed acyl derivatives of 1-benzylsemicarbazide, motivated by structural features associated in earlier studies with anticonvulsant activity, including benzyl, hydrazine, urea, and acyl-containing fragments. The authors prepared six 1-benzyl-4-acy…

Synthesis of p-iodo-N,N-di-(2-hydroxyethyl)aniline

A. N. NOVIKOV, A. M. SEDOV, Z. M. MURAV'EVA, N. P. POLISHCHUK
1975 SovietRxiv: ru-197501.12935

This paper reports the preparation of p-iodo-N,N-di-(2-hydroxyethyl)aniline, a hydroxyethylated iodoaniline not described in the cited literature and considered potentially useful as an intermediate for chloroethyl antitumor compounds. Two synthetic routes from p-iodoaniline were examined: reaction …

One-Step Synthesis of Iodonitro Derivatives of Benzene and Diphenyl

A. N. NOVIKOV, A. M. SEDOV
1975 SovietRxiv: ru-197501.12934

This paper addresses the preparation of iodonitro derivatives of benzene and diphenyl, noting that earlier routes required highly concentrated acids, multiple steps, or gave low yields. It proposes a one-stage synthesis based on the simultaneous action of iodine and a sulfuric, nitric acid mixture i…

On the Determination of Kinetic Parameters of Thermal Decomposition Processes of Solid Fuels from Derivatograms

S. I. Smolyaninov, V. I. Lozbin
1975 SovietRxiv: ru-197501.12931

This paper addresses the determination of kinetic parameters for thermal decomposition of solid fuels using derivatographic data, with attention to simplifying calculations from DTA, DTG, and TG curves. Assuming that decomposition of solid combustible minerals can often be formally described as a fi…

Investigation of the Effect of a Nonuniform Electrostatic Field on Heat Transfer and Flow Hydrodynamics

I. P. Chashchin, V. P. Ignatov, V. M. Madzurenko
1975 SovietRxiv: ru-197501.12930

This study examines how a nonuniform electrostatic field affects heat transfer and flow hydrodynamics in a vertical tube-in-tube heat exchanger with air flowing through the annular space under laminar conditions. Experiments varied air velocity and electrode voltage while measuring wall and air temp…

Studies on the Determination of Ultramicroimpurities in Complexing Agents

L. M. Poskrebysheva, A. A. Kaplin, B. A. Kubrak
1975 SovietRxiv: ru-197501.12929

This study addresses the need for highly sensitive control of heavy metal ultramicroimpurities in complexing agents used to clean semiconductor surfaces. The authors investigate amalgam polarographic determination of Cu, Pb, Cd, In, and Zn in morin and quinalizarin solutions using a mercury film cat…

Study of the Effect of Temperature on the Process of Preliminary Incorporation of Zirconium and Titanium Oxides into the Crystal Lattice of Alumina

V. M. VITYUGIN, V. V. KOYAIN, G. S. FROLOVA
1975 SovietRxiv: ru-197501.12928

This study examines how preliminary heat treatment temperature affects the incorporation of zirconium and titanium oxides into alumina-based charges, a factor considered important for the homogeneity and quality of alloyed corundums. Mixtures containing alumina with small additions of zirconium oxid…

Determination of the Unsaturation of 9-Vinylcarbazole

V. I. Berzin, E. E. Sirotkina, N. A. Ryzhova
1975 SovietRxiv: ru-197501.12927

A potentiometric method is proposed for determining the unsaturation, and hence monomer content, of 9-vinylcarbazole in colored or turbid solutions where existing analytical procedures are unsuitable. The method is based on rapid addition of mercury acetate to the vinyl group in methanol, with the e…

Rearrangement of N-Acetyldiphenylamine

E. E. SIROTKINA, R. M. KOGAN
1975 SovietRxiv: ru-197501.12926

The study examines the previously unsuccessful Fries-Rosenmund rearrangement of N-acetyldiphenylamine under acidic Lewis acid conditions. Using equimolar aluminum chloride and hydrogen chloride in several organic solvents, the authors found that the reaction proceeds intermolecularly to give diacety…

On the Composition of the Liquid Product of Synthesis from Carbon Monoxide and Water Vapor

S. I. Smolyaninov, A. V. Kravtsov, I. V. Goncharov
1975 SovietRxiv: ru-197501.12925

This study examines the composition of liquid products formed by synthesis from carbon monoxide and steam over an iron, copper catalyst at elevated pressures. Using distillation, chemical analysis, chromatography, and spectral studies, the authors compare product fractions and functional group compo…

Investigation of forsterite ceramics with a fine-crystalline structure

P. G. Usov, V. I. Vereshchagin, N. K. Glushkova
1975 SovietRxiv: ru-197501.12924

This study examines methods for improving the thermal shock resistance and mechanical strength of forsterite ceramics while preserving their dielectric properties. It investigates the formation of fine-crystalline forsterite from talc, talc products, and magnesium oxide, using small additions of str…

On the Synthesis and Sintering of Magnesium Aluminate Spinel

V. A. Amelina, V. I. Vereshchagin, P. G. Usov
1975 SovietRxiv: ru-197501.12923

This study examines solid-phase synthesis and sintering of magnesium aluminate spinel as a function of component ratio, mixing method, particle dispersity, firing temperature, atmosphere, and microadditives. X-ray phase analysis, shrinkage, water absorption, and lattice-parameter measurements were u…

Selection of the Optimal Granulation Mode for Superphosphate

V. M. Vityugin, T. G. Leont’eva, N. S. Shimitova, N. P. Kolosova
1975 SovietRxiv: ru-197501.12921

This study examines optimization of dish granulation conditions for superphosphate, addressing the low industrial yield of standard 1 to 5 mm granules. Using production samples from the Dzhambul superphosphate plant, the authors tested granulation on a 1 m dish granulator while varying dish inclinat…

On the Influence of Various Additives on the Thermal Stability of Green Iron Ore Pellets

T. G. Leont’eva, A. V. Vityugin
1975 SovietRxiv: ru-197501.12920

This study examines how bentonite, the polymeric structure-forming agent K-4, and lignin affect the pelletizing behavior and thermal stability of green iron ore pellets made from magnetite concentrate and related plant materials. Pellets prepared on a disk granulator from burdens with different addi…

Methods for Processing Pickling Solutions

S. A. Babenko, V. P. Pishchulin
1975 SovietRxiv: ru-197501.12919

This paper evaluates methods for treating spent ferric chloride etching solutions from printed circuit board production, containing iron and copper chlorides. Laboratory experiments compare copper recovery by cementation on iron shavings, ammoniacal processing with separation of iron hydroxides and …

On the Absorption of Metal Ions by Placer Minerals

S. A. Babenko
1975 SovietRxiv: ru-197501.12918

This study examines the sorption of selected heavy metal ions by placer minerals, focusing on ilmenite and zircon whose grain surfaces may carry clayey films capable of accumulating metals. Purified mineral fractions were exposed for two years to salt solutions, after which copper, lead, and zinc co…

Laboratory Setup for the Treatment of Acidic Wastewater

S. A. BABENKO, R. I. TASOEV, S. M. OLENEV
1975 SovietRxiv: ru-197501.12917

This paper describes the development and testing of a laboratory-scale continuous unit for treating acidic wastewater from electroplating and pickling operations containing heavy-metal ions and chromium compounds. Based on prior evaluation of treatment options, the proposed scheme mixes spent pickli…

Effect of Polymer Additives on the Hydraulic Resistance of Flow

I. P. CHASHCHIN; N. T. SHALAVIN, Yu. N. SUKHUSHIN
1975 SovietRxiv: ru-197501.12916

This paper examines how small polyethylene oxide additions affect hydraulic resistance in turbulent water flow through the annular channel of a tube-in-tube heat exchanger. Pressure drop, flow rate, and temperature were measured in a stabilized section over Reynolds numbers of about 10,000 to 40,000…

Study of Heat Transfer and Hydraulic Resistance of a Gas-Liquid Flow in a Tube-in-Tube Heat Exchanger

I. P. Chashchin, B. I. Litvinov, N. T. Shalavin
1975 SovietRxiv: ru-197501.12915

This paper reports an experimental study of heat transfer and hydraulic resistance in descending gas and gas-liquid flow through a vertical tube-in-tube heat exchanger. Air was passed through the annular space, with steam condensing in the inner tube, and subsequent two-phase tests introduced atomiz…

On the Relationship Between the Average Driving Forces of Cocurrent and Countercurrent Mass Transfer Processes

G. M. IZMAILOV
1975 SovietRxiv: ru-197501.12914

This paper examines the relation between mean driving forces in cocurrent and countercurrent mass transfer processes. It extends a standard proof, which required both operating and equilibrium lines to be linear, by retaining linear operating lines while allowing the equilibrium relation between pha…

Application of Direct Electric Heating for Concentrating Sulfuric Acid

V. P. PISHCHULIN
1975 SovietRxiv: ru-197501.12913

This paper examines direct electric heating as an alternative to furnace gas heating for concentrating sulfuric acid, with attention to reducing decomposition, entrainment, corrosion, and equipment bulk. It reports experimental measurements of specific boundary resistance in sulfuric acid solutions …

Improvement of the Chrome Electrocorundum Production Process Based on Determination of the Material and Heat Balances of Furnaces at the Yurga Abrasive Plant (YuAZ)

A. S. Bogma, I. P. Chashchin, N. A. Tikhonokova
1975 SovietRxiv: ru-197501.12909

This paper analyzes the production of chromium electrocorundum in electric arc furnaces at the Yurga Abrasives Plant through measured material and heat balances. It identifies causes of chemical heterogeneity and material loss, including imperfect charge preparation, segregation during transport and…

Effect of Quartz Raw Material Particle Size on the Kinetics of Silicon Carbide Formation

V. V. Shvetsov, V. M. Vityugin, V. I. Kosintsev
1975 SovietRxiv: ru-197501.12908

This study examines how the particle size of quartz raw material affects the kinetics of silicon carbide formation through the reaction of silica with carbon at 1460 to 1580°C. Gas evolution measurements were used to compare fine Tashlinsk sand, Glukhovets quartzite fractions, and two-layer quartz, …

Simultaneous Determination of Chromium and Iron in Corundum

A. V. Voznyak, V. V. Koyan
1975 SovietRxiv: ru-197501.12907

This paper examines chemical beneficiation of granular chromium electrocorundum contaminated with metallic chromium, iron, carbides, and related acid soluble impurities. Samples were boiled with hydrochloric acid of varying concentrations and treatment times, then separated into enriched corundum an…

New Ceramics for High-Frequency Technology

P. G. USOV, Z. S. KONOVALOVA, V. I. VERESHCHAGIN
1975 SovietRxiv: ru-197501.12906

This paper investigates ceramic materials for high-frequency technology based on the clinoenstatite to diopside compositional series. Minerals with varying calcium and magnesium oxide ratios were synthesized from both pure chemical reagents and natural raw materials, including talc and tremolite, us…

Application of the Thermal Quasi-Stationary Approximation Method to the Problem of Microlayer Evaporation

V. V. Salomatov, A. D. Gorbunov, A. V. Kuzmin
1975 SovietRxiv: ru-197501.12783

This paper develops an analytical treatment of evaporation in the thin liquid microlayer beneath a vapor bubble on a heated wall, a process important for bubble growth and boiling heat transfer. The authors formulate a one-dimensional Stefan-type heat conduction problem for the wall and microlayer a…

Unsteady Laminar Convection on a Radiating Plate

V. V. Salomatov, E. M. Puzyrev
1975 SovietRxiv: ru-197501.12782

This paper analyzes the interaction of thermal radiation with unsteady laminar boundary layers of a nonabsorbing fluid flowing over a heat-radiating plate under natural and forced convection. Using integral boundary-layer approximations, polynomial temperature and velocity profiles, and characterist…

Theory of the Mercury-Graphite Electrode

B. F. Nazarov, E. M. Mal’kov
1975 SovietRxiv: ru-197501.12781

This paper develops a theoretical description of electrochemical processes at a mercury graphite electrode formed by preliminary electrolysis, focusing on the kinetics and mechanism of mercury deposition on graphite. The authors model deposition as governed by nucleation and nucleus growth, deriving…

Thermal Decomposition of o-Iododiphenyl Dichloride

A. N. NOVIKOV, A. N. MOSKALCHUK, E. S. NOVIKOVA
1975 SovietRxiv: ru-197501.12780

This study examines the use of aryl iodide dichlorides as controllable chlorine sources for obtaining monochlorinated diphenyl derivatives, a reaction otherwise prone to di- and polychlorination with molecular chlorine. The authors prepared o-iododiphenyl, converted it nearly quantitatively to o-iod…

Kinetics and mechanism of direct iodination of aromatic compounds in acetic acid solution in the presence of nitric and sulfuric acids

A. M. SEDOV, A. N. NOVIKOV
1975 SovietRxiv: ru-197501.12779

The study examines the kinetics and probable mechanism of direct iodination of benzene in acetic acid in the presence of mixed nitric and sulfuric acids, using benzene as a model substrate to avoid side reactions. Iodine consumption was followed spectrophotometrically after extraction into carbon te…